采用BNi-5钎料钎焊K417G高温合金的界面组织和力学性能

周标, 王浩, 任新宇, 邱嘉玉, 潘晖

周标, 王浩, 任新宇, 等. 采用BNi-5钎料钎焊K417G高温合金的界面组织和力学性能[J]. 焊接, 2023(12):12 − 16. DOI: 10.12073/j.hj.20230523003
引用本文: 周标, 王浩, 任新宇, 等. 采用BNi-5钎料钎焊K417G高温合金的界面组织和力学性能[J]. 焊接, 2023(12):12 − 16. DOI: 10.12073/j.hj.20230523003
Zhou Biao, Wang Hao, Ren Xinyu, et al. Interfacial microstructure and mechanical properties of K417G superalloy brazed with BNi-5 brazing filler metal[J]. Welding & Joining, 2023(12):12 − 16. DOI: 10.12073/j.hj.20230523003
Citation: Zhou Biao, Wang Hao, Ren Xinyu, et al. Interfacial microstructure and mechanical properties of K417G superalloy brazed with BNi-5 brazing filler metal[J]. Welding & Joining, 2023(12):12 − 16. DOI: 10.12073/j.hj.20230523003

采用BNi-5钎料钎焊K417G高温合金的界面组织和力学性能

基金项目: 国家自然科学基金资助项目(52201050)
详细信息
    作者简介:

    周标,硕士,工程师;主要从事航空新材料焊接方向的研究;xiancai6278@163.com

  • 中图分类号: TG454

Interfacial microstructure and mechanical properties of K417G superalloy brazed with BNi-5 brazing filler metal

  • 摘要:

    K417G镍基高温合金具有优异的高温力学性能,可应用于航空发动机热端部件的制造中。采用BNi-5镍基钎料开展了K417G合金钎焊接头的研究,分析了不同保温时间对钎焊接头微观组织演变和接头高温力学性能的影响。在1160 ℃保温15 min条件下,K417G合金接头界面处物相主要由γ + γ'相、富Ti碳化物相和(Ni,Cr)3Si相等物相组成。随着保温时间的进一步延长,界面反应和元素扩散更为充分;同时接头中的硅化物相分布呈分散趋势,物相尺寸得到细化。1160 ℃ × 30 min条件下获得的接头950 ℃平均抗拉强度为412 MPa。

    Abstract:

    K417G nickel-based superalloy has excellent high-temperature mechanical properties and can be applied in the manufacturing of hot end components of aircraft engines. Brazed joints of K417G alloy were studied by BNi-5 nickel-based brazing filler metal. Effects of different holding time on microstructure evolution and high-temperature mechanical properties of brazed joints were analyzed. At 1160 ℃ for 15 mins, phases at interface of K417G alloy brazed joints were mainly composed of γ + γ' phase, Ti-rich carbide phase and (Ni,Cr)3Si phase. With the further extension of holding time, interfacial reaction and element diffusion became more sufficient. Meanwhile, distribution of silicide phase in brazed joints showed a dispersion trend, and phase size was refined. At 1 160 ℃ for 30 mins, average tensile strength of brazed joints at 950 ℃ was 412 MPa.

  • 图  1   钎焊接头高温拉伸试样

    图  2   1160 ℃ × 15 min钎焊接头微观组织

    图  3   图2b中钎缝中心和钎缝与母材界面局部组织

    图  4   1 160 ℃保温15 min,30 min,60 min接头组织及面分布情况

    图  5   不同保温时间下钎焊接头高温拉伸性能

    表  1   K417G高温合金成分(质量分数,%)

    CoCrMoAlTiFeVCNi
    9~118.5~9.52.5~3.54.8~5.74.1~4.7≤1.00.6~0.90.13~0.22余量
    下载: 导出CSV

    表  2   BNi-5钎料化学成分(质量分数,%)

    CrSiBCNi
    18.5~19.59.75~10.50≤0.03≤0.06余量
    下载: 导出CSV

    表  3   图2b中钎焊接头区域各微区能谱分析结果

    微区 元素含量(原子分数,%) 推测物相
    Al Si Ti V Cr Co Ni Mo
    1 15.18 0.21 5.53 0.63 9.88 8.67 58.00 1.90 母材γ + γ′相
    2 0.07 0.19 73.67 3.49 1.45 0.12 1.86 19.15 富Ti碳化物相
    3 12.11 6.54 3.67 0.57 10.94 6.43 58.49 1.25 近缝区γ + γ′相
    4 7.10 11.77 1.36 0.42 15.49 3.84 59.37 0.65 钎缝γ + γ′相
    5 0.39 28.56 8.64 0.40 8.63 1.91 48.46 3.01 (Ni,Cr)3Si相
    6 0.13 20.06 2.81 1.53 33.97 1.52 30.08 9.90 (Ni,Cr)3Si相
    7 14.11 1.68 4.79 0.69 9.89 8.62 58.39 1.83 近缝区γ + γ′相
    8 0 0.01 74.72 3.30 1.40 0.13 1.35 19.09 富Ti碳化物相
    下载: 导出CSV
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出版历程
  • 收稿日期:  2023-05-22
  • 网络出版日期:  2023-12-10
  • 刊出日期:  2023-12-10

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