工艺参数对Fe-Mn-Cr-N钢搅拌摩擦加工微观组织和力学性能的影响

Effect of processing parameters on microstructure and mechanical properties of Fe-Mn-Cr-N steel during friction stir processing

  • 摘要:
    目的 旨在研究Fe-Mn-Cr-N在高应变速率和大应变变形条件下的组织细化机理。
    方法 通过搅拌摩擦加工工艺试验对Fe-Mn-Cr-N奥氏体不锈钢进行表面处理,转速为600~800 r/min,加工速度为50~70 mm/min。利用OM和EBSD等方法分析不同参数下的加工区域形貌和再结晶行为,并利用显微硬度仪和万能试验机进行力学性能研究。
    结果 结果表明,除600 r/min-60 mm/min参数外,其他参数加工的Fe-Mn-Cr-N钢都获得无缺陷的加工表面,焊核区组织由原始粗大的柱状晶粒细化为约10 μm的均匀等轴晶粒,加工区域微观组织由大量高角度晶界、丰富的低角度晶界和Σ3孪晶界组成。在600 r/min-50 mm/min参数下加工的Fe-Mn-Cr-N钢具有最佳的综合力学性能,其屈服强度和抗拉强度由原始材料的211.4 MPa和421.2 MPa增加到400.9 MPa和649.0 MPa。
    结论 试验结果可为含氮奥氏体不锈钢的表面强化技术提供工艺参数和数据支撑。

     

    Abstract: Objective The purpose was to study refinement mechanism of microstructure of Fe-Mn-Cr-N under high strain rate and large strain deformation conditions. Methods The surface treatment of Fe-Mn-Cr-N austenitic stainless steel was carried out by friction stir processing technology. Rotation speed was 600~800 r/min and processing speed was 50~70 mm/min. OM and EBSD were used to analyze morphology and recrystallization behavior of the processed area under different parameters, and the mechanical properties were studied by microhardness tester and universal testing machine. Results The results showed that the surface of Fe-Mn-Cr-N steel was flawless except 600 r/min-60 mm/min, and microstructure of welding nugget zone was refined from the original coarse columnar grain to about 10 μm uniform grain. Microstructure of the processed area was composed of a large number of high angle grain boundaries, abundant low angle grain boundaries and Σ3 twin grain boundaries. Fe-Mn-Cr-N steel processed at 600 r/min-50 mm/min had the best comprehensive mechanical properties, whose yield strength and tensile strength increased from 211.4 MPa and 421.2 MPa to 400.9 MPa and 649.0 MPa of the original material. Conclusion The experimental results could provide technical parameters and data support for surface strengthening technology of austenitic stainless steel containing nitrogen.

     

/

返回文章
返回