Mg-Gd-Nd-Zr镁合金大尺寸缺陷被动填充式搅拌摩擦修复

Passive filling friction stir repairing of Mg-Gd-Nd-Zr magnesium alloy large-sized defect

  • 摘要:
    目的 旨在研究Mg-Gd-Nd-Zr镁合金板被动填充式搅拌摩擦修复(Passive filling friction stir repairing, PFFSR)试样微观组织与力学性能,以期为工程应用提供理论参考。
    方法 该文采用PFFSR分别对Mg-Gd-Nd-Zr镁合金直径10 mm,20 mm和40 mm,深5 mm的大尺寸缺陷进行修复并利用光学显微镜、扫描电镜、能谱分析仪和电子背散射衍射仪修复试样微观组织表征,利用显微硬度计和万能试验机对修复试样进行力学性能测试。
    结果 结果表明,PFFSR能够有效消除3种尺寸缺陷,修复区与基板实现了致密的冶金连接。剧烈塑性变形和动态再结晶的耦合作用使修复区的晶粒尺寸显著细化并且使第二相弥散分布,平均晶粒尺寸从母材的39.2 μm细化至2.1 μm,细晶强化显著改善了修复区的性能,重叠界面由于重复的PFFSR热力循环造成晶粒长大和第二相粗化。修复区的平均硬度为73 HV,10 mm直径缺陷修复后抗拉强度为224 MPa,达到母材的85.2%;断后伸长率为13.2%,较母材提高到240%。由于缺陷尺寸增加,导致修复时间增加热输入提高,使得修复后的断后伸长率下降,但抗拉强度仍保持稳定。缺陷尺寸的增加至20 mm和40 mm时,断后伸长率分别为9.4%和7.7%。
    结论 PFFSR能够实现3种大尺寸缺陷修复后抗拉强度均达到母材85%以上,为镁合金构件的修复提供了一种高效、可靠的方法。

     

    Abstract: Objective This study aims to investigate microstructure and mechanical properties of Mg-Gd-Nd-Zr magnesium alloy plates repaired by passive filling friction stir repairing (PFFSR), in order to provide theoretical reference for engineering applications. Methods In this paper, PFFSR was employed to repair large-size defects (with diameters of 10 mm, 20 mm, and 40 mm, and a depth of 5 mm) in Mg-Gd-Nd-Zr magnesium alloy. Microstructure of the repaired samples was characterized by optical microscopy, scanning electron microscopy, energy dispersive spectroscopy and electron backscatter diffraction. Mechanical properties were evaluated through microhardness testing and universal testing machine measurements. Results The results demonstrate that PFFSR effectively eliminates defects across three different sizes, achieving a dense metallurgical bonding between repaired zone and base plate. The coupling effect of severe plastic deformation and dynamic recrystallization significantly refines grain structure and promotes dispersion of the second phase. The average grain size is refined from 39.2 μm in base metal to 2.1 μm, leading to notable grain refinement strengthening in the repaired zone. However, grain growth and coarsening of the second phase are observed at overlapping interfaces due to repeated PFFSR thermal–mechanical cycles. The average microhardness of the repaired zone reaches 73 HV. After repairing a 10 mm diameter defect, tensile strength reaches 224 MPa, representing 85.2% that of base metal, while elongation increases significantly to 13.2%, 240% that of base metal. With increasing defect size (20 mm and 40 mm), prolonged processing and higher heat input results in a decrease in elongation to 9.4% and 7.7%, respectively, though tensile strength remains stable. Conclusion PFFSR can achieve tensile strength over 85% that of base metal after repairing three types of large-sized defects, providing an efficient and reliable method for repairing magnesium alloy components.

     

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